| Résumé | Ultrasonic diagnosing technique with a new high-temperature ultrasonic transducer is developed to real-time diagnose polymer processing and its morphology changes in injection molding processing. Compared with the previous researches, the new technique can provide more and accurate information. In this study, ultrasound diagnosis shows that longitudinal wave can real-time characterize the data of the injection process and polymer morphology changes, including melt flow arrival time, the part ejection time, filling and packing stages, polymer solidification process, and the morphology changes during polymer crystallization. Shear waves can real-time diagnose Young's and shear storage modulus, anisotropy property of polymer in injection molding. During our research, real-time ultrasonic diagnosis shows that the storage modulus along the vertical direction is larger than that of the parallel to the melt flow direction under our setup injection conditions. Scanning electron microscopy and dynamic mechanical analysis measurements present that it is because the crystalline lamellas of HDPE are parallel arrangement and grow in a vertical to melt flow direction owing to injection shear force under a certain injection conditions. |
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