| DOI | Resolve DOI: https://doi.org/10.4028/www.scientific.net/MSF.727-728.873 |
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| Author | Search for: Halmenschlager, Cibele Melo1; Search for: KorbRoberto, Maita De Angelis; Search for: Neagu, Roberto1; Search for: Bergmann, Carlos Pérez; Search for: Malfatti, Célia de Fraga |
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| Affiliation | - National Research Council of Canada. Energy, Mining and Environment
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| Format | Text, Article |
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| Conference | 8th International Latin-American Conference on Powder Technology, November 6-9, 2011, Florianópolis, Brazi |
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| Subject | Dense thin films; Different substrates; Heat treatment process; Nano-structured; Oxidization; Precursor solutions; Pyrolysis process; Salt dissolution; Solvent influence; YSZ thin films; Glycerol; Scanning electron microscopy; Solid oxide fuel cells (SOFC); Spray pyrolysis; Thermoanalysis; X ray diffraction; Yttria stabilized zirconia; Yttrium; Zirconia; Zirconium; Vapor deposition |
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| Abstract | The development of solid oxide fuel cell with thin film concepts for an electrode supported design based on the yttria-stabilized zirconia has demonstrated favourable results due to its high chemistry stability in oxidization and environment reduction. The spray pyrolysis process was investigated in order to obtain dense thin films of YSZ on different substrates. The precursor solution was obtained by zirconium and yttrium salt dissolutions in a mixture of water and glycerine in several ratios to study the solvent influence. The substrate was initially heated at 600 °C and during the deposition it ranged from 260-350°C, finishing at a fast increase in temperature of 600°C. The heat treatment was carried out in four different temperatures: 700 °C, 750 °C, 800 °C, and 900 °. The precursors were characterized by thermal analysis. The microstructures of the films were studied using scanning electron microscopy and X-ray diffraction. The results obtained showed that the films obtained were crystalline before the heat treatment process and have shown ionic conductivity above 800°C. |
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| Publication date | 2012-08-24 |
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| In | |
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| Language | English |
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| Peer reviewed | Yes |
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| NPARC number | 21270234 |
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| Export citation | Export as RIS |
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| Report a correction | Report a correction (opens in a new tab) |
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| Record identifier | 1e40f8ca-fb38-4229-89e5-4af2ee3d8e72 |
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| Record created | 2014-01-14 |
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| Record modified | 2020-04-21 |
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